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KMID : 1024419970010030233
Food Engineering Progress
1997 Volume.1 No. 3 p.233 ~ p.239
The Effects of Operation Variables on the Efficiency of Supercritical Fluid Extraction of Fatty Acids from Fish Oil
Noh Duck-Woo

Goo Gyoung-Mo
Hur Byung-Ki
Abstract
Eicosapentaenoic acid (EPA) and Docosahexaenoic acid (DHA) were ex¥ðacted from the mixture of fatty acids, which is composed of from 12 to 22 carbons, by the Supercritical F1uid Extraction (SFE) process. In
this study, the relation nong the extraction characteristics of EP A and DHA such a<; extraction temperature,
flow rate and volume of CO2 fluid, and working pressure was investigated. ¥ðle concentrations of EP A and
DHA in the extract increased with both the de¥áease of flow rate of C02 and the reduction of volume CO2
used for the extraction. Therefore, the solubility data at equilibrium were obtained by extrapolating these
results to the zero of flow rate of CO2 and to the zero of volume of CO2? At constant temperature, the solubilities of EPA and DHA in a super.¥áiti 1 fluid increased rapidly with pressure. ¥ðtis occurs because of the
rapid rise in the density. At constant extraction pressure, the solubility of various fatty acids decreased with
the increase of temperature and showed a minimum value at a particular temperature. ±îlIs phenomena, what
is called retrograde condensation, wa<; occurred in the region of 300
C to 50o
C, and nonretrograde condensation took place from 500
C up.
KEYWORD
eicosapentaenoic acid, docosahexaenoic acid, supercritical fluid extraction, retrograde condensation, nonretrograde condensation
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